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In this way a reduction of the operating temperature can be observed, thus reducing the power consumption of devices, while keeping the catalytic performance of the material.In the current work, we report the on-chip fabrication of a low-temperature H₂S sensor based on p-type Co₃O₄ nanofibers (NFs) using the electrospinning method. The FESEM images show the typical spider-net like morphologies of synthesized Co₃O₄ NFs with an average diameter of 90 nm formed on the comb-like electrodes. The EDX data indicate the presence of Co and O elements in the NFs. The XRD analysis results confirm the formation of single-phase cubic spinel nanocrystalline structures (Fd3 m) for the synthesized Co₃O₄ NFs. The Raman results are in agreement with the XRD data through the presence of five typical vibration modes of the nanocrystalline Co₃O₄. The gas sensing properties of the fabricated Co₃O₄ NF sensors are tested to 1 ppm H₂S within a temperature range of 150 °C to 450 °C. The results indicate a highest sensor response to 1 ppm H₂S with the gas response of aproximately 2.1 times and the gas response/recovery times of 75 s/258 s at a low temperature of 250 °C. The fabricated sensor also demonstrates good selectivity and a low detection limit of 18 ppb. The overall results suggest a simple and effective fabrication process for the p-type Co₃O₄ NF sensor for practical applications in detecting H₂S gas at low temperature.Zinc oxide (ZnO) is a well-known semiconductor with valuable characteristics wide direct band gap of ˜3.3 eV, large exciton binding energy of 60 meV at room temperature, high efficient photocatalyst, etc. which have been applied in many fields such as optical devices (LEDs, laser), solar cells and sensors. Besides, various low dimensional structures of ZnO in terms of nanoparticles, nanorods, nanoneedles, nanotetrapods find applications in technology and life. This material is also appealing due to the diversity of available processing methods including both chemical and physical approaches such as hydrothermal, sol-gel, chemical vapor deposition and sputtering. In this report, ZnO nanorods are prepared by hydrothermal method assisted with galvanic-cell effect. The effect of counter electrode materials on the morphology and structure of obtained product was studied. https://www.selleckchem.com/mTOR.html Scanning electron microscopy (SEM) images of the product showed that counter electrodes made of aluminum offers nanorods of higher quality than other materials in terms of uniform size, high density and good preferred orientation. The as-prepared nanorods were then sputtered with gold (Au). ZnO/Au nanostructures show excellent photocatalyst activities which were demonstrated by complete photodegradation of methylene blue (Mb) under UV irradiation and high decomposition rate k of 0.011 min-1.An efficient, simple, environment-friendly and inexpensive cupric oxide (CuO) electrocatalyst for oxygen evolution reaction (OER) is demonstrated. CuO is chemically deposited on the porous carbon material obtained from the dehydration of common sugar. The morphology of CuO on the porous carbon material is plate-like and monoclinic crystalline phase is confirmed by powder X-ray diffraction. The OER activity of CuO nanostructures is investigated in 1 M KOH aqueous solution. To date, the proposed electrocatalyst has the lowest possible potential of 1.49 V versus RHE (reversible hydrogen electrode) to achieve a current density of 20 mA/cm₂ among the CuO based electrocatalysts and has Tafel slope of 115 mV dec-1. The electrocatalyst exhibits an excellent long-term stability for 6 hours along with significant durability. The enhanced catalytic active centers of CuO on the carbon material are due to the porous structure of carbon as well as strong coupling between CuO-C. The functionalization of metal oxides or other related nanostructured materials on porous carbon obtained from common sugar provides an opportunity for the development of efficient energy conversion and energy storage systems.A new solid solution, (1-x)Bi0.5Na0.5TiO₃+xBaCoO3-δ materials, was fabricated using the sol-gel method. X-ray diffraction showed that the crystal structure of the compound exhibited rhombohedral symmetry and is similar to the crystal structures of host Bi0.5Na0.5TiO₃ materials. Distortions in the structures and reduction in the optical band gaps of the Bi0.5Na0.5TiO₃ materials were possibly due to the random incorporation of Ba and Co cations into host lattice materials. The magnetic properties of the Bi0.5Na0.5TiO₃ materials were tuned by controlling the concentrations of BaCoO3-δ as the solid solution. We expect that our work will provide valuable information on current methods for integrating ferromagnetic properties into lead-free ferroelectric materials for the development of multiferroic materials.Designing a nanocomposite with sensitive and selective determination of ascorbic acid is challenging task. It is possible through the exploitation of attractive features of nanoscience and nanotechnology for the synthesis of nanostructured materials. Herein, we report the decoration of nanoparticle of MoS x on the surface of Co₃O₄ nanowires by hydrothermal method. The MoS x nanoparticles shared the large surface on the Co₃O₄ nanowires, thus it supported in the development enzyme free ascorbic acid sensor. Non-enzymatic sensor based on MoS x -Co₃O₄ composite was found very selective for the determination of ascorbic acid (AA) in phosphate buffer solution of pH 7.4. The MoS x -Co₃O₄ nanocomposite was used to modify the glassy carbon electrode to measure AA from variety of practical samples. The MoS x -Co₃O₄ nanocomposite was used to modify the glassy carbon electrode and it has shown the attractive analytical features such as a low working potential +0.3 V, linear range of concentration from 100-7000 μM, low limit of detection 14 μM, and low limit of quantification (LOQ) of 42 μM. The developed sensor is highly selective and stable. Importantly, it was applied successfully for the practical applications such as detection of AA from grapefruit, tomato and lemon juice. The excellent electrochemical properties of fabricated MoS x -Co₃O₄ nanocomposite can be attributed to the increasing electro active surface area of MoS x . The presented nanocomposite is earth abundant, environment friendly and inexpensive and it holds promising features for the selective and sensitive determination of AA from practical applications. The nanocomposite can be capitalized into the wide range of biomedical applications.
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